Synfacts

Issue 11 · November 2012

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A107
SYNFORM ISSUE 2012/11 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
z1163
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1163
Synthesis of (+)-Artemisinin

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1164
Second-Generation Synthesis of Sulopenem

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1165
Third-Generation Synthesis of Sulopenem

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1166
Convergent Total Syntheses of Callipeltosides A, B, and C

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1167
Synthesis of (–)-9-epi-Presilphiperfolan-1-ol and (–)-Presilphiperfolan-1-ol

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1168
Synthesis of an H₃ Antagonist

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1169
Synthesis of MK-4256

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1170
Synthesis of a Hydroxamic Acid LpxC Inhibitor

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1171
Synthesis of (+)-Ponapensin and (+)-Elliptifoline

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1172
Synthesis of Methopholine

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1173
Total Synthesis of (+)-Marinomycin A

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1174
Synthesis of a BACE1 Inhibitor

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1175
Synthesis of (–)-Jiadifenin

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1176
Synthesis of AM-8553

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1177
Second-Generation Synthesis of (–)‑Aplyviolene

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1178
Synthesis of an IGF-1R Modulator

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1179
Synthesis of Thiazesim

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Synthesis of Heterocycles
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1181
Rhodium/Lewis Acid Catalyzed Cascade Synthesis of Tetrahydropyridazines

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1182
Heterocycles via Use of 2-Heteroaryl-2-(tetrahydrofuranyliden)acetonitriles

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1183
Practical Brønsted Acid Mediated Synthesis of Coumarins from Allenes

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1184
Cu-Catalyzed Synthesis of Furoindolines from Tryptophols

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1185
Synthesis of Isoindolinones by an Asymmetric Aza-Wacker-type Cyclization

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1186
Silver-Catalyzed Heteroannulation Route to 1-Aminoisoquinolines

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1187
One-Pot Gold-Catalyzed Synthesis of Azepino[1,2-a]indoles

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1188
Cascade Synthesis of 3-Pyrrolines by a Heck–Aza-Michael Reaction

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1189
Expedient Route to Complex Alkaloids through Pd(II)-Catalyzed Indole C-2 Alkylation

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1190
Synthesis of Iodotriazoles Using in Situ Generated Electrophilic Triiodide

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1191
One-Pot Asymmetric Synthesis of 4-Hydroxypyrazolidines from Aldehydes

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1192
Direct C-2 Pyridine C–H Olefination

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Synthesis of Materials and Unnatural Products
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1193
Efficient, Non-Toxic Polylactide Synthesis

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1194
Synthesis of New Ladder Diboroles

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1195
Ketenimine Intermediates in the Pot

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1196
Cycloparaphenylenes by the Gram

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1197
Iterative Synthesis of Polyynes

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1198
Gram-Scale Synthesis of an Antiaromatic Porphyrinoid

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1199
Naphthalenes by Microwave-Assisted Dehydrogenative Diels–Alder Reaction

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1200
Tetrathiafulvalene-Based Microporous Metal-Organic Framework

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1201
One-Step Access to Luminescent Pentaaryldiazaboroles

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1202
From Masked Diazonium Salts to Boronic Esters

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1203
Controlled Radical Polymerization by Turning on the Lights

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1204
Fusing π-Conjugated Heterocycles

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1205
Mechanical Stress Yields HCl

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z1207
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1207
Asymmetric Conjugate Addition of Phosphines to Ene-Imines

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1208
Cu-Catalyzed Asymmetric Cyclopropanation of 1,2-Disubstituted Alkenes

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1209
Iridium-Catalyzed Enantioconvergent Thioetherification

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1210
Rhodium-Catalyzed Enantioselective Nucleophilic Allylation of Imines

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1211
Dehydrogenative Heck Reaction Using Rh(III)

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1212
Platinum-Catalyzed Hydrative Cycloisomerization

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1213
Iridium-Catalyzed Asymmetric Hydrogenation of α-Substituted Acrylic Acids

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1214
Asymmetric Epoxidation of Conjugated Olefins with Dioxygen

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1215
Enantioselective Synthesis of Tertiary α-Hydroxyketones

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1216
Diastereoselective Cyclohexyl- and Tetrahydropyranyl Syntheses by Nickel Catalysis

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1217
Asymmetric Pyrrolidine Synthesis by [3+2] Cycloaddition of α-Silylimines

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1218
All-Carbon Macrocycles by Catalytic Gosteli–Claisen Rearrangement

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1219
Asymmetric Epoxidation with an Iron–Porphyrin-like Complex

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1220
Ruthenium-Catalyzed Asymmetric Transfer Hydrogenation of Ketones

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1221
Ruthenium NHC-Catalyzed Z- and Enantioselective Cross-Metathesis

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1222
C–H Activation and E-Double Bond Formation by Ruthenium Catalysis

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1223
Asymmetric ipso-Friedel–Crafts Alkylation for Quaternary Spirocenters

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1224
Iridium-Catalyzed Enantioselective Hydrogenation of Sulfones

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1225
Oxazaborolidinium Ion Catalyzed Asymmetric Roskamp Reaction

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1226
Iridium-Catalyzed Enantioselective Hydrogenation of Isoquinolines

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1227
Ir(I)-Catalyzed Asymmetric Hydrogenation of Seven-Membered Cyclic Imines

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1228
Synthesis of Chiral 1,1-Diarylethanes by Stereospecific Nickel Catalysis

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1229
Ruthenium-Catalyzed Asymmetric Hydrogenation of Imines

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1230
Copper-Catalyzed Asymmetric Claisen Rearrangement of Enolphosphonates

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1231
Enantioselective Co-Catalysis to Trap Reactive Zwitterionic Intermediates

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1232
β,β-Disubstituted Nitroalkene Hydrogenation Using Rhodium

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1233
Palladium-Catalyzed Stereoselective Direct Substitution of Allylic Amines

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1234
Rhodium(II) Carbenoids for Alkynoate Synthesis

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1235
N,N′-Dioxide Scandium Catalyzed Enantioselective Friedel–Crafts Reaction

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1236
Asymmetric Ring-Expansion of Isatins

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Metal-Mediated Synthesis
z1237
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1237
Fe-Catalyzed sp³–sp³ Cross–Coupling

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1238
Synthesis of 8-Oxabicyclo[3.2.1]octanes by Cationic Cascade Cyclization

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1239
Cu(I)-Catalyzed Addition of Nucleophilic Silicon to Propargylic Derivatives

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1240
Enantioselective Ti(III)-Catalyzed Reductive Cyclization of Ketonitriles

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1241
Palldium-Catalyzed Synthesis of Dihydrocycloocta[b]indoles from Iodoindoles

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1242
Iron-Mediated Hydrofluorination of Unactivated Alkenes

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1243
Stereodivergent Synthesis of Tri- and Tetrasubstituted Alkenes

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1244
Double Addition of Grignard Reagents to Acyl Cyanhydrins

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1245
Fe-Catalyzed Diastereoselective Cross-Coupling of Cyclic Halohydrins

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1246
Fluoroform-Derived CuCF₃ for Trifluoromethylation of Arylboronic Acids

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1247
Functionalized 2-Aryloxetanes by Oxetane-Directed ortho-Lithiation

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1248
Copper-Mediated Cyanation of Indoles and 2-Phenylpyridines

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1249
Diastereoselective Addition of Arylzinc Reagents to Sugar Aldehydes

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1250
Aryl Carbamates and Sulfamates as Reagents in Fe-Catalyzed Couplings

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1251
Trifluoromethylation of Propargylic Derivatives Using (Ph₃P)₃Cu(CF₃)

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Organo- and Biocatalysis
z1253
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1253
Asymmetric Vinylogous Conjugate Additions of γ-Substituted Butenolides

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1254
Cinchona Alkaloid-Catalyzed Isomerization of Imines

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1255
Organocatalytic Asymmetric Synthesis of Prostaglandin PGF_2α

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1256
Catalytic Asymmetric Oxyfluorination of Enamides

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1257
H-Bond-Directed Trienamine Catalysis

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1258
Superbase-Initiated Mannich Reactions of Sulfonylimidates

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1259
Primary Amine Catalyzed Enantioselective Friedel–Crafts Alkylation of Enones

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1260
NHC-Catalyzed Enantioselective Synthesis of β,γ-Unsaturated α-Fluoroesters

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1261
Catalytic Asymmetric Conjugate Addition of Aldehydes to Acrylates

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Polymer-Supported Synthesis
z1263
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1263
A³-Coupling Reaction with Au@PMO-IL

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1264
Asymmetric Amination with a Polymer-Supported Chiral Rhodium Complex

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1265
Borylation of N-Adjacent C(sp³)–H Bonds with Silica-TRIP/Rh

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1266
A SiO₂-Supported Pd–Amine Catalyst for the Tsuji–Trost Reaction

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1267
Monolith-Supported Flow Synthesis of 2-Aminopyrimidines

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1268
Au NPs-Catalyzed Oxidation of Hydrosilanes to Silanols

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1269
A Clay-Supported Cu(II) Catalyst for the One-Pot Synthesis of Aryl Triazoles

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1270
Carbonylative Cyclization of Halobenzoic Acids with PS-NHC–Pd

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1271
A Silica-Supported Trifluoromethyl Ketone with KHSO₅ for Epoxidation

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1272
Epoxidation of Olefins with a Peracid Supported on Silica

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1273
Annulation of Quinone Monoacetals with Alkenes Using PS-PFBA

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1274
Preparation of Aminoimidazopyridines with γ-Fe₂O₃@SiO₂-OSO₃H

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1275
Chemoselective Hydrogenation of Carbonyls with Ni–Sn/AlOH

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Addenda and Errata
1277
Bottom-up Synthesis of Zigzag Carbon Nanotube Belt Precursors

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1278
Fe-Catalyzed Oxyamination of Alkenes with N-Sulfonyl Oxaziridines

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