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Synlett 2001; 2001(10): 1578-1580
DOI: 10.1055/s-2001-17461
DOI: 10.1055/s-2001-17461
letter
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Enantioselective Allyltitanation and Cross-Metathesis. Synthesis of (-)-Prosophylline
Further Information
Publication History
Publication Date:
27 September 2001 (online)
An enantioselective synthesis of (-)-prosophylline has been accomplished in 15 steps from protected d-glyceraldehyde, with an overall yield of 9.2%, by using two enantioselective allyltitanations and a cross-metathesis reaction as the key-steps.
enantioselective allylation - alkaloids - cross-metathesis - piperidines - (-)-prosophylline