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Synlett 1997; 1997(7): 803-804
DOI: 10.1055/s-1997-5774
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Palladium Catalyzed Reaction of Bis(triisopropylsilyl)disulfide with Acetylenes

Yves Gareau* , Arturo Orellana
  • *Merck Frosst Centre for Therapeutical Research, C.P. 1005, Pointe Claire-Dorval, Québec, Canada, H9R 4P8
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Publication History

Publication Date:
31 December 2000 (online)

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The cross-coupling reaction of Bis(triisopropylsilyl)-disulfide on acetylenes yielded 1,2-alkylthioolefins after deprotection with TBAF and quenched with an electrophile.

disulfide - palladium coupling - alkyne

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