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Synthesis 1997; 1997(6): 668-672
DOI: 10.1055/s-1997-1391
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New Applications of Dimethyl Pentacyclo[6.4.0.02,10.03,7.04,9]dodeca-5,11-diene-8,9-dicarboxylate in the Synthesis of Polycyclic Compounds

Pelayo Camps* , Oscar Coll, Francesc Pérez, Santiago Vázquez
  • *Laboratori de Química Farmacéutica, Facultat de Farmàcia, Universitat de Barcelona, Av. Diagonal s/n; E-08028 Barcelona, Spain, Fax +34(3)4021886; E-mail: camps@farmacia.far.ub.es
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Publication Date:
31 December 2000 (online)

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A short synthesis of diester 9 and the first synthesis of dimethyl 8,9-dihydrotriquinacene-2,6-dicarboxylate (10 from the readily available pentacyclic diester 1 is described.

dimethyl tetracyclo[5.2.1.02,6.03,8]decane-7,8-dicarboxylate - dimethyl 8,9-dihydrotriquinacene-2,6-dicarboxylate - iodosobenzene diacetate - 2,2'-dithiopyridine 1,1'-dioxide - oxidative decarboxylation/fragmentation

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