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Synlett 1995; 1995(7): 707-708
DOI: 10.1055/s-1995-5046
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Synthesis of Methacryloylamides, -ureas, -carbamates, and Dihydropyrimidine-2,4-diones from Hex-1-en-2-yl Methacrylate

Bénédicte Seiller* , Christian Bruneau1 , Pierre H. Dixneuf1
  • *Laboratoire de Chimie de Coordination Organique, URA CNRS 415, Campus de Beaulieu, Université de Rennes, F-35042 Rennes, France
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Publication History

Publication Date:
31 December 2000 (online)

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Methacryloylamides, -ureas and -carbamates have been synthesized by acylation of amides, ureas and carbamates with hex-1-en-2-yl methacrylate prepared via ruthenium catalysis. On reaction with primary amines, butyl N-methacryloylcarbamate gives a ready access to dihydropyrimidine-2,4-diones.

ruthenium catalysis - hex-1-en-2-yl methacrylate - acylamides - acylureas - acylcarbamates - dihydropyrimidine-2,4-diones

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