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Synlett 1992; 1992(6): 499-501
DOI: 10.1055/s-1992-21392
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Thiosilanes in Organic Synthesis: A Novel Approach to Vinyl Sulphides

Alessandro Degl'lnnocenti* , Paola Ulivi, Antonella Capperucci, Alessandro Mordini, Gianna Reginato, Alfredo Ricci
  • *Centro C.N.R. sulla Chimica e la Struttura dei Composti Eterociclici e loro Applicazioni, via G. Capponi 9,I-50121 Firenze, Italy
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Publication Date:
08 March 2002 (online)

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Silyl enol ethers 1 react under the influence of diethyl ether-boron trifluoride complex with silylated sulphides to afford a new and general access to a wide range of vinyl sulphides 2. When α,β-unsaturated ketones are used, a mild synthesis of 1,3-bis(phenylthio)propenes 6 is achieved.

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