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Synlett 1990; 1990(11): 713-714
DOI: 10.1055/s-1990-21223
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A New Synthetic Method for 3-Halocyclopentenes via Thermal Conversion of Cycloadducts of Dihalocarbenes with Dicyclopentadiene

A. B. Kostitsyn* , E. V. Shulishov, Yu. V. Tomilov, O. M. Nefedov
  • *N. D. Zelinksy Institute of Organic Chemistry, Academy of Sciences USSR, Leninsky prospect 47, Moscow B-334, USSR
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Publication Date:
08 March 2002 (online)

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Vacuum thermolysis of readily available 4,4-dihalotetracyclo [6.2.1.02,7.03,5]undec-9-enes, prepared from the addition of dihalocarbenes to endo-tricyclo[5.2.1.02,6]deca-3,8-diene under phase-transfer catalysis, affords 3-halocyclopentenes in high yield (70-80%).

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