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Synthesis 1989; 1989(6): 461-463
DOI: 10.1055/s-1989-27290
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Reactions of Terminal Alkynes with Bis(trimethylsilyl) Peroxide and Zinc(II) Iodide: A Convenient Method for the Preparation of 1-Iodo-1-alkynes

A. Ricci* , M. Taddei, P. Dembech, A. Guerrini, G. Seconi
  • *Centro sulla Chimica e la Struttura dei Composti Eterociclici e loro Applicazioni del C.N.R., c/o Dipartimento di Chimica Organica Dell'Università, Via G. Capponi 9, I-50121 Firenze, Italy
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Publication Date:
17 September 2002 (online)

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A convenient, mild, and general one-pot synthesis of 1-iodo-1-alkynes from terminal acetylenes, bis(trimethylsilyl) peroxide, and zinc(II) iodide in the presence of n-butyllithium is reported.

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