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Synthesis 1988; 1988(10): 790-792
DOI: 10.1055/s-1988-27708
DOI: 10.1055/s-1988-27708
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Convenient One-Pot Conversion of Alcohols into Esters via Hemiacetal Intermediates
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Publication History
Publication Date:
12 September 2002 (online)
A simple and efficient one-pot oxidative procedure, adaptable to a large scale, is described for the preparation of methyl esters from either primary alcohols or vic-diols. The aldehyde is generated by Swern or periodate oxidation, followed by bromine oxidation of the methyl hemiacetal formed in aqueous methanolic solution.