Download PDF
Synthesis 1987; 1987(6): 555-557
DOI: 10.1055/s-1987-28001
communication
© Georg Thieme Verlag, Rüdigerstr. 14, 70469 Stuttgart, Germany. All rights reserved. This journal, including all individual contributions and illustrations published therein, is legally protected by copyright for the duration of the copyright period. Any use, exploitation or commercialization outside the narrow limits set by copyright legislation, without the publisher's consent, is illegal and liable to criminal prosecution. This applies in particular to photostat reproduction, copying, cyclostyling, mimeographing or duplication of any kind, translating, preparation of microfilms, and electronic data processing and storage.

A New Method for the Preparation of Bis(1-hydroxyalkyl)-phosphinic Acids

Piotr Majewski*
  • *Institute of Organic Chemistry, Technical University (Politechnika), Żwirki 36, PL-90-924 Łódź 40, Poland
Further Information

Publication History

Publication Date:
20 August 2002 (online)

  PDF Download  Permissions and Reprints All articles of this category

Bis(1-hydroxyalkyl)phosphinic acids 6 have been conveniently obtained by addition of bis(trimethylsiloxy)phosphine 1 to aldehydes or ketones 2 in the presence of chlorotrimethylsilane and triethylamine, followed by ethanolysis of the resulting trimethylsilyl bis(1-trimethylsiloxyalkyl)-phosphinales 5.

      >