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Synthesis 1987; 1987(6): 554-555
DOI: 10.1055/s-1987-28000
DOI: 10.1055/s-1987-28000
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A Convenient and Facile Synthesis of Dialkylphosphines
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Publication History
Publication Date:
20 August 2002 (online)
A series of simple dialkylphosphines 2 has been prepared by the thermal disproportionation of dialkylphosphine oxides 1 induced by the R2P(O)Cl/R2PCl system, generated in situ from 1 with a catalytic amount of carbon tetrachloride.