DOI:
10.1055/s-00000083
Synlett
LinksClose Window
References
For 3f, see: Candiano G, Bruschi M, Musante L, Santucci L, Ghiggeri GM, Carnemolla B, Orecchia P, Zardi L, Righetti PG.
Electrophoresis 2004;
25: 1327 (R)-2-O-Acetyl-2-(2-nitrophenyl)acetonitrile (3d): 1H NMR (400 MHz, CDCl3) δ 2.21 (s, 3 H), 7.09 (s, 1 H), 7.68 (dt, J = 8.2, 1.4 Hz, 1 H), 7.80 (dt, J = 7.7, 1.3 Hz, 1 H), 7.93 (dd, J = 7.8, 1.2 Hz, 1 H), 8.20 (dd, J = 8.2, 1.2 Hz, 1 H). 13C NMR (150 MHz, CDCl3): δ 20.1, 59.6, 115.0, 125.8, 129.3, 131.3, 134.5, 147.0, 168.3. IR (Neat): 3123, 3036, 2333, 1756, 1399, 1116, 1064 cm–1. HRMS: m/z [M + H]+ calcd for C10H9O4N2: 221.0557; found: 221.0547
Access:
We do not assume any responsibility for the contents of the web pages of other providers.