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DOI: 10.1055/s-2006-950059
Low Molecular Weight Polyphenols in insect infected leaves of Quercus ilex L. (Fagaceae)
Plant-insect interactions in Mediterranean ecosystems have not hitherto sufficiently studied in terms of Chemical Ecology. Quercus ilex is an excellent model for this type of study, as its leaves present impressive alterations after insect attacks.
In this study, low molecular weight polyphenols were studied by HPLC in samples of insect infected leaves. The leaves were extracted with solvents of increasing polarity and the methanol extract was further submitted to chromatographic separations, mainly column chromatography and HPLC and afforded gallic, protocatechuic, vanillic, caffeic, ferulic, and ellagic acids. Comparative HPLC study of healthy and infected leaves showed an increase in the phenolic content. The structures of the isolated compounds were established by means of 1D & 2D NMR.