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Synthesis 1994; 1994(7): 683-684
DOI: 10.1055/s-1994-25545
short paper
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Efficient Synthesis of 3-Aminothioacrylamides by Iminoformylation of Thioacetamides

Andreas Rolfs* , Jürgen Liebscher
  • *Fachbereich Chemie, Humboldt-Universität Berlin, Hessische Str. 1-2, D-10115 Berlin, Germany
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Publication Date:
17 September 2002 (online)

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Heating substituted thioacetamides 1 with either trismorpholinomethane or with a mixture of triethyl orthoformate and a secondary amine gives high yields of synthetically versatile 3-aminothioacryl-amides 4.

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