One Step α-Deoxygenation of Unprotected Aldonolactones using Samarium Diiodide-THF/H2O System - A New Synthesis of 2-Deoxy-D-Ribose

Stephen Hanessian; Christian Girard

doi:10.1055/s-1994-23034

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Synlett 1994; 1994(10): 861-862
DOI: 10.1055/s-1994-23034

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One Step α-Deoxygenation of Unprotected Aldonolactones using Samarium Diiodide-THF/H₂O System - A New Synthesis of 2-Deoxy-D-Ribose

Stephen Hanessian^* , Christian Girard

^*Department of Chemistry, Université de Montréal, P.O.Box 6128, Station A, Montréal, (Québec), H3C 3J7, CANADA

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Publication Date:
22 March 2002 (online)

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The use of SmI₂ in THF/H₂O system effects a straightforward α-deoxygenation reaction of unprotected tetrono- and pentonolactones providing a facile access to their 2-deoxy analogs.

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